Synthesis and crystal structure of N-ethyl-N-cytisinocarbothioamide

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dc.contributor.authorTurdybekov, K. M.
dc.contributor.authorNurkenov, O. A.
dc.contributor.authorTurdybekov, D. M.
dc.contributor.authorSatpaeva, Zh. B.
dc.contributor.authorFazylov, S. D.
dc.date.accessioned2022-04-28T05:48:56Z
dc.date.available2022-04-28T05:48:56Z
dc.date.issued2021
dc.description.abstractBased on (–)-cytisine alkaloid and ethyl isothiocyanate, N-ethyl-N-cytisinocarbothioamide is synthesized and its structure is proved by 1H NMR spectroscopy and single crystal X-ray diffraction. The mesomeric effect is shown in the carbothioamide group formed. It is found that π-conjugation between nitrogen atoms and the thiocarbonyl group is weakened due to the steric hindrance between hydrogen atoms of the piperidine ring and the thioamide group.ru_RU
dc.identifier.citationSynthesis and crystal structure of N-ethyl-N-cytisinocarbothioamide/K. M.Turdybekov[et al.]//Journal of Structural Chemistry.-2021.-Vol62(11).-pp.1791-1796ru_RU
dc.identifier.issn0022-4766
dc.identifier.urihttps://rep.buketov.edu.kz//handle/data/12490
dc.publisherJournal of Structural Chemistryru_RU
dc.relation.ispartofseriesJournal of Structural Chemistry;Vol62(11)
dc.subjectalkaloidsru_RU
dc.subjectcytisineru_RU
dc.subjectcarbothioamideru_RU
dc.subjectethyl isothiocyanateru_RU
dc.subjectNMR spectroscopyru_RU
dc.subjectsingle crystal X-ray diffractionru_RU
dc.titleSynthesis and crystal structure of N-ethyl-N-cytisinocarbothioamideru_RU
dc.typeArticleru_RU

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